4-氯-N-2-丙烯-1-基-苯胺合成路线 （共 16 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Jain, Seema; Pandey, Neelesh; Kishore
Journal of the Indian Chemical Society, 2006 , vol. 83, # 10 p. 1052 - 1054
反应条件
in 1,2-dichloro-ethane T=70°C; 24 h; Sealed tube;
参考文献
Symeonidis, Theodoros S.; Lykakis, Ioannis N.; Litinas, Konstantinos E.
Tetrahedron, 2013 , vol. 69, # 23 p. 4612 - 4616
反应条件
titanium(IV) isopropylate; MS 4 Angstroem; palladium diacetate; triphenylphosphine in benzene T=80°C; Alkylation; N-allylation; 3 h;
参考文献
Yang, Shyh-Chyun; Hung, Chung-Wei
Synthesis, 1999 , # 10 p. 1747 - 1752
反应条件
potassium fluoride on Celite in acetonitrile Reflux;
参考文献
Kumar, Subodh; Kaur, Pervinder
Tetrahedron Letters, 2004 , vol. 45, # 17 p. 3413 - 3416
反应条件
potassium carbonate; thiophenol in N,N-dimethyl-formamide T=40°C; 4 h;
参考文献
Rassadin, Valentin A.; Tomashevskiy, Aleksandr A.; Sokolov, Viktor V.; Ringe, Arne; Magull, Joerg; De Meijere, Armin
European Journal of Organic Chemistry, 2009 , # 16 p. 2635 - 2641
反应条件
indium; sodium iodide in N,N-dimethyl-formamide T=20°C; Barbier allylation; 3 h;
参考文献
Yadav; Madhuri; Reddy; Reddy, G. S. Kiran Kumar; Sabitha
Synthetic Communications, 2002 , vol. 32, # 18 p. 2771 - 2777
反应条件
1: pyridine-2-carbaldehyde; 4-chloro-aniline in tetrahydrofuran; water T=30°C; 2 h; 2: allyl bromide With indium in tetrahydrofuran; water T=30°C; Barbier allylation; 5 h; Further stages.;
参考文献
Kumar, Subodh; Kaur, Pervinder
Tetrahedron Letters, 2004 , vol. 45, # 17 p. 3413 - 3416
反应条件
1.1: NaH / tetrahydrofuran / 0.5 h / 0 °C 1.2: tetrahydrofuran / 16 h / Heating 2.1: aq. HCl / tetrahydrofuran / 16 h / Heating View Scheme
参考文献
Mondal, Poulomi; Thander, Latibuddin; Chattopadhyay, Shital K.
Tetrahedron Letters, 2012 , vol. 53, # 11 p. 1328 - 1331
反应条件
NaY T=130°C; 5.83333 h;
参考文献
Selva; Tundo; Perosa
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 677 - 680
反应条件
1.1: Et3N / tetrahydrofuran / 14 h / 20 °C 2.1: NaH / tetrahydrofuran / 0.5 h / 0 °C 2.2: tetrahydrofuran / 16 h / Heating 3.1: aq. HCl / tetrahydrofuran / 16 h / Heating View Scheme
参考文献
Yip, Kai-Tai; Yang, Min; Law, Ka-Lun; Zhu, Nian-Yong; Yang, Dan
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3130 - 3131
