2,4,6-三甲氧基苯硼酸合成路线 (共 3 条)
反应条件
1: With n-butyllithium in tetrahydrofuran T=0°C; 2 h; Inert atmosphere; 2: With boric acid trimethyl ester in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; 3: With water in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Dennis, Eric G.; Jeffery, David W.; Perkins, Michael V.; Smith, Paul A.
Tetrahedron, 2011 , vol. 67, # 11 p. 2125 - 2131
反应条件
bis-triphenylphosphine-palladium(II) chloride; water; sodium hydroxide in tetrahydrofuran T=70°C; 24 h; Inert atmosphere;
参考文献
Dennis, Eric G.; Jeffery, David W.; Perkins, Michael V.; Smith, Paul A.
Tetrahedron, 2011 , vol. 67, # 11 p. 2125 - 2131
反应条件
bis-triphenylphosphine-palladium(II) chloride; water; sodium hydroxide in tetrahydrofuran T=70°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 67, # 11 p. 2125 - 2131