3-氯-2,2-二甲基丙酸合成路线 （共 26 条）
反应条件
tetrachloromethane; sulfuryl dichloride; dibenzoyl peroxide
参考文献
US2302228 , ;
Journal of the American Chemical Society, , vol. 62, p. 928
反应条件
boron trifluoride T=100°C;
参考文献
Journal of Organic Chemistry, , vol. 11, p. 785
参考文献
US2302228 , ;
Journal of the American Chemical Society, , vol. 62, p. 928
反应条件
im UV-Licht(λ:365.5nm);
参考文献
Bulletin des Societes Chimiques Belges, , vol. 61, p. 366,374
反应条件
thionyl chloride Heating;
参考文献
Okawara; Matsuda; Noguchi; Furukawa
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1574 - 1578
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Okawara, Tadashi; Matsuda, Takashi; Furukawa, Mitsuru
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1225 - 1233
反应条件
sodium in chloroform
参考文献
Teijin Ltd.
Patent: US3950361 A1, 1976 ;
反应条件
sodium sulfide; sodium carbonate
参考文献
Feeder, Neil; Ginnelly, Michael J.; Jones, Ray V. H.; O'Sullivan, Susan; Warren, Stuart; Wyatt, Paul
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 22 p. 3479 - 3483
反应条件
1: 89 percent / Na2CO3, Na2S / H2O / 45 °C 2: 92 percent / conc. H2SO4 / benzene / 24 h / Heating View Scheme
参考文献
De Almeida, Gabriela; Sletten, Ellen M.; Nakamura, Hitomi; Palaniappan, Krishnan K.; Bertozzi, Carolyn R.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 10 p. 2443 - 2447
反应条件
1: Na2S*9H2O; sodium carbonate / water / 24 h / 45 - 50 °C 2: sulfuric acid / benzene / 24 h / Reflux 3: sodium / toluene / 24 h / Inert atmosphere; Reflux 4: bromine / tetrachloromethane / 0.75 h / 20 °C View Scheme
参考文献
King, Mathias; Baati, Rachid; Wagner, Alain
Chemical Communications, 2012 , vol. 48, # 74 p. 9308 - 9309
