sulfuryl dichloride T=20°C; 1 h;

sodium carbonate in decane 1 h; Heatingother thiocarbonates; Product distribution;

sodium carbonate in decane 1 h; Heatingother thiocarbonates; Product distribution;

Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1900508', constants.ctx, '0')">carbon monoxide</a>; <a href="#" onclick="return RXDsubstances(event, this, '969616', constants.ctx, '0')">phenol</a> <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '4921294', constants.ctx, '0')">sulfur</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '508906', constants.ctx, '0')">1,8-diazabicyclo[5.4.0]undec-7-ene</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=80&deg;C;&nbsp;P=7500.6&nbsp;Torr;&nbsp;6&nbsp;h;&nbsp;<br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '969135', constants.ctx, '0')">methyl iodide</a> &nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=20&deg;C;&nbsp;P=750.06&nbsp;Torr;&nbsp;16&nbsp;h;&nbsp;<br /> &nbsp;

Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1730824', constants.ctx, '0')">dimethyl-disulfide</a> <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11323438', constants.ctx, '0')">AlCl₃, aluminium chloride</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '8973685', constants.ctx, '0')">zinc</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />T=80&deg;C;&nbsp;1.5&nbsp;h;&nbsp;<br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '606778', constants.ctx, '0')">phenyl chloroformate</a> &nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />T=80&deg;C;&nbsp;1&nbsp;h;&nbsp;<br /> &nbsp;

Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1697284', constants.ctx, '0')">carbon oxide sulfide</a>; <a href="#" onclick="return RXDsubstances(event, this, '969616', constants.ctx, '0')">phenol</a> <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '508906', constants.ctx, '0')">1,8-diazabicyclo[5.4.0]undec-7-ene</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=20&deg;C;&nbsp;P=750.06&nbsp;Torr;&nbsp;1&nbsp;h;&nbsp;<br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '969135', constants.ctx, '0')">methyl iodide</a> &nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=20&deg;C;&nbsp;P=750.06&nbsp;Torr;&nbsp;2&nbsp;h;&nbsp;<br /> &nbsp;

&nbsp;1) 1,4-dioxane, DMSO, r.t., 40 min, 2) 24 h;&nbsp;&nbsp;Yield given. Multistep reaction;&nbsp;<br /> &nbsp;