反-N-苄氧羰基-4-羟基-L-脯氨酸合成路线 (共 36 条)
反应条件
sodium hydrogencarbonate in diethyl ether Acylation;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 16 p. 1845 - 1847
反应条件
sodium hydrogencarbonate in water; toluene
反应条件
triethylsilane; trifluoroacetic acid in dichloromethane 0.583333 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 33, # 37 p. 5441 - 5444
反应条件
sodium hydrogencarbonate in water; toluene
反应条件
1: With sodium hydroxide; methanesulfonyl chloride in CPME; water T=80 - 105°C; 4 - 6 h; 2: With sodium hydroxide in CPME; water T=20 - 65°C; 2 - 8 h;
参考文献
JP2005/112761 A, ;
Page/Page column 8 ;
反应条件
in dichloromethane T=20°C; 16 h;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 62, # 11 p. 1459 - 1464
反应条件
sodium tris(acetoxy)borohydride
参考文献
Tetrahedron Letters, , vol. 45, # 32 p. 6097 - 6100
反应条件
1: 94 percent / SOCl2 2: 60 percent / PPh3; DIAD / tetrahydrofuran 3: 90 percent / NaN3 / dimethylformamide 4: 93 percent / H2; Ni / ethyl acetate 5: 98 percent / methanol; Pd/C View Scheme
参考文献
Umashankara; Babu, I Ramesh; Ganesh, Krishna N
Chemical communications (Cambridge, England), 2003 , # 20 p. 2606 - 2607
反应条件
1: dicyclohexylcarbodiimide; THF 2: palladium; aqueous HCl / Hydrogenation View Scheme
参考文献
Folk; Burstone
Archives of Biochemistry, 1956 , vol. 61, p. 257,258
反应条件
1: CrO3 2: NaBH4 3: HBr, AcOH 5: 1) DAST, 2) RuO4 6: 1) HCl, 2) Ag2O View Scheme
参考文献
Hudlicky, Milos
Journal of Fluorine Chemistry, 1991 , vol. 54, # 1-3 p. 195