4’-氯-[1,1’-联苯]-4-胺合成路线 （共 17 条）
反应条件
sodium hydroxide in water T=75°C;
参考文献
US2013/338369 A1, ;
Paragraph 0243; 0244; 0343; 0344; 0345; 0346; 0347-0349 ;
反应条件
sodium hydroxide in water T=75°C;
参考文献
US2013/338369 A1, ;
Paragraph 0243; 0244; 0355; 0356; 0357; 0358; 0359-0368 ;
反应条件
potassium carbonate in ethanol; water T=65°C; Suzuki-Miyaura Coupling; 4 h;
参考文献
Tong, Jinhui; Wang, Haiyan; Cai, Xiaodong; Zhang, Qianping; Ma, Hengchang; Lei, Ziqiang
Applied Organometallic Chemistry, 2014 , vol. 28, # 2 p. 95 - 100
反应条件
potassium carbonate in ethanol T=78°C; Suzuki-Miyaura coupling; 12 h; Air atmosphere;
参考文献
Zhou, Bo; Li, Yi-Qun
E-Journal of Chemistry, 2011 , vol. 8, # 4 p. 1490 - 1497
反应条件
oxygen; sodium hydroxide in water T=60°C; 33 h; regioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 79, # 5 p. 2314 - 2320
反应条件
manganese(IV) oxide in acetonitrile T=20°C; Overall yield = 54 percent; regioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 77, # 23 p. 10699 - 10706
反应条件
platinum on activated charcoal; ethanol; hydrazine hydrate
参考文献
Journal of the Chemical Society, , p. 4265,4269
反应条件
1: hydrogenchloride; sodium nitrite / water; acetic acid / 1 h / 0 °C 2: manganese(IV) oxide / acetonitrile / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 77, # 23 p. 10699 - 10706
反应条件
PPA; trifluoroacetic acid T=20°C; Substitution; decomposition; trifluoroacetylation; 3 h; Further byproducts. Title compound not separated from byproducts.;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 2 p. 295 - 300
反应条件
1: HNO3 2: Sn, aq. HCl View Scheme
参考文献
Helvetica Chimica Acta, , vol. 62, p. 185 - 197
