N-(2,5-二甲氧基苯基) 苯甲酰胺合成路线 （共 5 条）
反应条件
potassium phosphate; C43H59NO2PPd(1+)*CH3O3S(1-) in tert-butyl alcohol T=110°C; 1.5 h; Inert atmosphere; Reagent/catalyst;
参考文献
Bruno, Nicholas C.; Buchwald, Stephen L.
Organic Letters, 2013 , vol. 15, # 11 p. 2876 - 2879
反应条件
triethylamine in dichloromethane T=0 - 20°C; 1 h;
参考文献
Nawrat, Christopher C.; Lewis, William; Moody, Christopher J.
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7872 - 7881
反应条件
1: 89 percent / HNO3; H2O / acetic acid / 1.5 h / 20 °C 2: 79 percent / Lawesson's reagent / toluene / 12 h / 80 °C 3: 100 percent / HCO3(-) / methanol / 24 h / Heating View Scheme
参考文献
Jackson, Yvette A.; Lyon, Michael A.; Townsend, Norman; Bellabe, Kettyna; Soltanik, Fernando
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 2 p. 205 - 210
反应条件
1: 89 percent / HNO3; H2O / acetic acid / 1.5 h / 20 °C 2: 89 percent / tin; HCl / aq. ethanol / 3 h / Heating View Scheme
参考文献
Jackson, Yvette A.; Lyon, Michael A.; Townsend, Norman; Bellabe, Kettyna; Soltanik, Fernando
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 2 p. 205 - 210
反应条件
1: 90 percent / Lawesson's reagent / toluene / 2 h / 80 °C
2: 80 percent / NaOH, K3<Fe(CN)6> / H2O / 24 h / Ambient temperature
3: 90 percent / ceric ammonium nitrate / acetonitrile; H2O / 1 h / Ambient temperature
View Scheme
参考文献
Lyon, Michael A.; Lawrence, Simon; Williams, David J.; Jackson, Yvette A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 4 p. 437 - 442
