反应条件
1: 82 percent / PPh3*Br2 / acetonitrile 2: 1.) Na / 1.)diglyme 2.) diglyme 140 deg C, 2h 3: 40percent aq NaOH / H2O; ethanol / 4 h / Ambient temperature 4: 1.5 M HCl / bis-(2-methoxy-ethyl) ether / 1 h / 120 °C View Scheme
参考文献
Kuklev; Popkov; Kas'yanov; Akulin; Bezuglov
Russian Journal of Bioorganic Chemistry, 1996 , vol. 22, # 3 p. 192 - 195
