反应条件
THF in tetrahydrofuran; cyclohexane to WCl5 under N2 cyclohexane was added, mixt. was stirred, THF was added, mixt. was allowed to cool under N2 for 1 h; filtered, dried in vac., washed with cyclohexane and n-pentane;
参考文献
Rice, C. A.; Benson, C. G.; McAuliffe, C. A.; Hill, W. E.
Inorganica Chimica Acta, 1982 , vol. 59, p. 33 - 40
