N,N-二甲基-2-苯氧基乙胺合成路线 (共 16 条)
反应条件
HPtCl6·6H2O; 1,1,3,3-tetramethyldisiloxane in tetrahydrofuran; toluene T=50°C; 5 h; Inert atmosphere;
参考文献
Hanada, Shiori; Tsutsumi, Emi; Motoyama, Yukihiro; Nagashima, Hideo
Journal of the American Chemical Society, 2009 , vol. 131, # 41 p. 15032 - 15040
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether in toluene T=20°C; Inert atmosphereReflux;
参考文献
Hamid, M. Haniti S. A.; Allen, C. Liana; Lamb, Gareth W.; Maxwell, Aoife C.; Maytum, Hannah C.; et al.
Journal of the American Chemical Society, 2009 , vol. 131, p. 1766 - 1774
反应条件
in acetonitrile T=180°C; 5 h; Autoclave;
参考文献
Arico, Fabio; Chiurato, Matteo; Peltier, Josephine; Tundo, Pietro
European Journal of Organic Chemistry, 2012 , # 17 p. 3223 - 3228
反应条件
sodium hydride in diethyl ether; N,N-dimethyl-formamide 15 h; Ambient temperature;
参考文献
Wada, Akimori; Kanatomo, Shoichi; Nagai, Sotoo
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1016 - 1022
反应条件
sodium; copper(I) bromide 2.) NMP, reflux, 1.5 h; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 48, # 17 p. 3633 - 3652
反应条件
ethanol T=80 - 90°C;
参考文献
Yakugaku Zasshi, , vol. 63, p. 387,389
Chem.Abstr., , p. 3350
反应条件
potassium hydroxide; ethanol T=130°C;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 497, p. 171,175, 178
反应条件
1: 56 percent / benzene; H2O / Ambient temperature 2: 69 percent / LiAlH4 / diethyl ether / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 68, # 3 p. 135 - 137
反应条件
1: 5.5 g / SOCl2 / 16 h / Ambient temperature 2: 56 percent / benzene; H2O / Ambient temperature 3: 69 percent / LiAlH4 / diethyl ether / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 68, # 3 p. 135 - 137
反应条件
2: acetone View Scheme
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 39, p. 1529 - 1533,1430 - 1433