in gas
High Pressure; reagents added to tube in dry ice bath, sealed in amts. to develop about 30-50 atm of pressure at 300°C, heated at 310-350°C for 1.5-69 h; analyzed by GLC;
参考文献
Scaduto, Patricia M.; Speier, John L.
Inorganic Chemistry, 1983 , vol. 22, p. 3363 - 3364
in neat (no solvent)
quiet electric discharges on a H2 stream with the mixture of SiCl4- and Br2-vapors, passed through a discharge tube;; mixture obtained;;
参考文献
Besson, A.; Fournier, L.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1911 , vol. 152, p. 603 - 605