in water mixing components solns. (small amount of NH3OH-salt), water removal (distn.) to dryness; no isolation in pure state; IR spectroscopy;
参考文献
Titova, K. V.; Kolmakova, E. I.; Rosolovskii, V. Ya.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1978 , vol. 23, p. 634 - 636
Zhurnal Neorganicheskoi Khimii, 1978 , vol. 23, p. 1146 - 1149
Titova, K. V.; Kolmakova, E. I.; Rosolovskii, V. Ya.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1978 , vol. 23, p. 634 - 636
Zhurnal Neorganicheskoi Khimii, 1978 , vol. 23, p. 1146 - 1149
in ethanol -70 to -60°C, storing (120 h), gradual increase of temperature; IR spectroscopy;
参考文献
Titova, K. V.; Loginova, E. N.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1995 , vol. 40, p. 1714 - 1720
Zhurnal Neorganicheskoi Khimii, 1995 , vol. 40, p. 1781 - 1787
slow dehydration of small amt. of comp. to avoid expolosion;
参考文献
Titova, K. V.; Loginova, E. N.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1995 , vol. 40, p. 1714 - 1720
Zhurnal Neorganicheskoi Khimii, 1995 , vol. 40, p. 1781 - 1787
Dresler, W. F. C.; Stein, R.
Liebigs Annalen der Chemie, 1869 , vol. 150, p. 242 - 252
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Gmelin Handbook: C: MVol.D1, 34.7.4, page 343 - 344
