4,4’-双(溴甲基)-2,2’-联吡啶合成路线 （共 13 条）
反应条件
sulfuric acid; hydrogen bromide 6 h; Reflux;
参考文献
Li, Yinan; Liu, Yifan; Nam, Dayoung; Park, Sungnam; Yoon, Juyoung; Hyun, Myung Ho
Dyes and Pigments, 2014 , vol. 100, # 1 p. 241 - 246
反应条件
1,2-dibromo-1,1,2,2-tetrafluoroethane; cesium fluoride in N,N-dimethyl-formamide T=25°C; 2 h;
参考文献
Fraser, Cassandra L.; Anastasi, Natia R.; Lamba, Jaydeep J. S.
Journal of Organic Chemistry, 1997 , vol. 62, # 26 p. 9314 - 9317
反应条件
sulfuric acid; hydrogen bromide Substitution; 6 h; Heating;
参考文献
Will, Geoffrey; Boschloo, Gerrit; Rao, S. Nagaraja; Fitzmaurice, Donald
Journal of Physical Chemistry B, 1999 , vol. 103, # 38 p. 8067 - 8079
反应条件
1: 99 percent / conc. H2SO4 / 60 h / Heating 2: 30 percent / NaBH4 / methanol / 60 h / Heating 3: 30 percent / aq. HBr / 3.5 h / Heating View Scheme
参考文献
Liu, Ken-Yen; Ko, Chih-Yang; Ho, Kuo-Chuan; Lin, King-Fu
Polymer, 2011 , vol. 52, # 15 p. 3318 - 3324
反应条件
1: 30 percent / NaBH4 / methanol / 60 h / Heating 2: 30 percent / aq. HBr / 3.5 h / Heating View Scheme
参考文献
Liu, Ken-Yen; Ko, Chih-Yang; Ho, Kuo-Chuan; Lin, King-Fu
Polymer, 2011 , vol. 52, # 15 p. 3318 - 3324
反应条件
hydrogen bromide in water 3 h; Heating;
参考文献
Ashton, Peter R.; Balzani, Vincenzo; Credi, Alberto; Kocian, Oldrich; Pasini, Dario; Prodi, Luca; Spencer, Neil; Stoddart, J. Fraser; Tolley, Malcolm S.; Venturi, Margherita; White, Andrew J. P.; Williams, David J.
Chemistry - A European Journal, 1998 , vol. 4, # 4 p. 590 - 607
反应条件
1: NaBH4; aq. NaOH / methanol / 1 h / 20 °C 2: aq. HBr; H2SO4 / Heating View Scheme
参考文献
Prakasam, Thirumurugan; Lusi, Matteo; Elhabiri, Mourad; Platas-Iglesias, Carlos; Olsen, John-Carl; Asfari, Zouhair; Cianferani-Sanglier, Sarah; Debaene, Francois; Charbonniere, Loic J.; Trabolsi, Ali
Angewandte Chemie - International Edition, 2013 , vol. 52, # 38 p. 9956 - 9960
Angew. Chem., 2013
反应条件
1: 89 percent / NaBH4 / ethanol / 3 h / 20 °C 2: 88 percent / HBr; H2SO4 / 6 h / Heating View Scheme
参考文献
Chandrasekharam; Srinivasarao; Suresh; Reddy, M. Anil; Raghavender; Rajkumar; Srinivasu; Reddy, P. Yella
Journal of Chemical Sciences, 2011 , vol. 123, # 1 p. 37 - 46
反应条件
1: 43.5 percent / acetic acid / 4 h / Heating 2: 44 percent / NaOH; water / methanol / 3 h / Heating 3: 72.3 percent / hydrobromic acid / 5 h / Heating View Scheme
参考文献
Ward, Robert S.; Branciard, Denis; Dignan, Rosemary A.; Pritchard, Martyn C.
Heterocycles, 2002 , vol. 56, # 1-2 p. 157 - 170
反应条件
1: 44 percent / NaOH; water / methanol / 3 h / Heating 2: 72.3 percent / hydrobromic acid / 5 h / Heating View Scheme
参考文献
Ward, Robert S.; Branciard, Denis; Dignan, Rosemary A.; Pritchard, Martyn C.
Heterocycles, 2002 , vol. 56, # 1-2 p. 157 - 170
