1,2-二溴-1,2-二苯基乙烷合成路线 (共 45 条)
反应条件
maghemite(γ-Fe2O3) nanoparticle supported 2,2'-bis[3-(triethoxysilyl)propyl]imidazolium substituted diethyl ether bis(tribromide) in methanol; dichloromethane 4 h; Reflux;
参考文献
European Journal of Inorganic Chemistry, , # 36 p. 6156 - 6163
反应条件
2,2'-azo-bisisobutyronitrile; bromine in tetrachloromethane T=65°C; 2 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 56, # 10 p. 3323 - 3329
反应条件
[bis(acetoxy)iodo]benzene; potassium bromide in dichloromethane; water T=20°C; 0.25 h;
参考文献
Synthetic Communications, , vol. 39, # 2 p. 220 - 227
反应条件
polylt;styrene-co-(4-vinylpyridinium salt)gt; (R = n-C6H13) in dichloromethane T=23°C; 4.5 h; Yields of byproduct given;
参考文献
Tetrahedron, , vol. 46, # 17 p. 6161 - 6166
反应条件
polylt;styrene-co(4-vinylpyridinium salt)gt;(R = n-C6H13) in dichloromethane T=23°C; 20 h; Yields of byproduct given;
参考文献
Tetrahedron, , vol. 46, # 17 p. 6161 - 6166
反应条件
Sodium bromate; sulfuric acid; sodium bromide in 1,4-dioxane; water T=20°C; 7 h;
参考文献
Tetrahedron Letters, , vol. 50, # 21 p. 2529 - 2532
反应条件
tetra-n-butylammonium tribromide in chloroform T=20°C; 1 h;
参考文献
Canadian Journal of Chemistry, , vol. 64, p. 603 - 607
反应条件
N-bromosuccinmide; trimethylsilylazide; 4 A molecular sieve; zinc trifluoromethanesulfonate in dichloromethane T=0°C; 1 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 47, # 39 p. 7017 - 7019
反应条件
1: With orthosilicic acid tetramethyl ester; diphenyl[2-(triethoxysilyl)ethyl]phosphine; (3-(2-aminoethylamino)-propyl)-trimethoxysilane in n-heptane T=80°C; Wittig condensation; 12 h; 2: With pyridinium hydrobromide perbromide in n-heptane T=80°C; 8 h;
参考文献
Tetrahedron Letters, , vol. 48, # 2 p. 293 - 295
反应条件
sodium dithionite; 1,1'-di-n-octyl-4,4'-bipyridinium dibromide in water; ethyl acetate 48 h; two-phase system;
参考文献
Journal of the American Chemical Society, , vol. 106, # 21 p. 6217 - 6222