2-乙氧基-4,5,6,7-四氢-3H-氮杂卓合成路线 （共 16 条）
反应条件
1: 75 percent / 20 h / 140 - 145 °C
2: 79 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating
3: 70 percent / Heating
View Scheme
参考文献
Shukla, U. K.; Khanna, J. M.; Sharma, Satyavan; Anand, Nitya; Chatterjee, R. K.; Sen, A. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 664 - 668
反应条件
1: 75 percent / 20 h / 140 - 145 °C
2: 79 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating
3: 70 percent / Heating
4: 57 percent / LiAlH4
5: 88 percent / NaHCO3 / dimethylformamide / Heating
View Scheme
参考文献
Shukla, U. K.; Khanna, J. M.; Sharma, Satyavan; Anand, Nitya; Chatterjee, R. K.; Sen, A. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 664 - 668
反应条件
1: 75 percent / 20 h / 140 - 145 °C
2: 79 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating
3: 70 percent / Heating
4: 57 percent / LiAlH4
5: 50 percent / NaHCO3 / dimethylformamide / Heating
View Scheme
参考文献
Shukla, U. K.; Khanna, J. M.; Sharma, Satyavan; Anand, Nitya; Chatterjee, R. K.; Sen, A. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 664 - 668
反应条件
1: 75 percent / 20 h / 140 - 145 °C
2: 79 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating
3: 70 percent / Heating
4: 57 percent / LiAlH4
5: 90 percent / benzene / Ambient temperature
View Scheme
参考文献
Shukla, U. K.; Khanna, J. M.; Sharma, Satyavan; Anand, Nitya; Chatterjee, R. K.; Sen, A. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 664 - 668
反应条件
1: 75 percent / 20 h / 140 - 145 °C
2: 79 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating
3: 70 percent / Heating
4: 57 percent / LiAlH4
View Scheme
参考文献
Shukla, U. K.; Khanna, J. M.; Sharma, Satyavan; Anand, Nitya; Chatterjee, R. K.; Sen, A. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 664 - 668
反应条件
dicobalt octacarbonyl in ethylene glycol dimethyl ether
T=100°C; P=51714.8 Torr; 48 h;
参考文献
Xu, Hongyu; Jia, Li
Organic Letters, 2003 , vol. 5, # 21 p. 3955 - 3957
