sodium hydride in tetrahydrofuran T=20°C; Wittig reaction; 5 h;
参考文献
Sun, Bin; Hoshino, Juma; Jermihov, Katie; Marler, Laura; Pezzuto, John M.; Mesecar, Andrew D.; Cushman, Mark
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 14 p. 5352 - 5366
1: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane T=0°C; Wittig type reaction; 2: 3,4,5-trimethoxy-benzyl alcohol With 4,4'-di-tert-butylbiphenyl; lithium; nickel dichloride in tetrahydrofuran; hexane Wittig type reaction; 48 h; Inert atmosphereReflux;
参考文献
Alonso, Francisco; Riente, Paola; Yus, Miguel
European Journal of Organic Chemistry, 2009 , # 34 p. 6034 - 6042