N-(2,3-二甲基苯基)乙酰胺合成路线 （共 30 条）
反应条件
sulfuric acid; water
1.) 35-40 deg C; 2.) 6 h, 90 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Courtin, Alfred; Tobel, Hans-Rudolf von
Helvetica Chimica Acta, 1980 , vol. 63, # 2 p. 385 - 394
反应条件
sulfuric acid; nitric acid
T=0°C; 1 h;
参考文献
Havlik, Martin; Kral, Vladimir; Kaplanek, Robert; Dolensky, Bohumil
Organic Letters, 2008 , vol. 10, # 21 p. 4767 - 4769
反应条件
sulfuric acid; nitric acid
参考文献
Noelting; Braun; Thesmar
Chemische Berichte, 1901 , vol. 34, p. 2255
反应条件
1: HNO3, H2SO4
2: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, aq. CuSO4
View Scheme
参考文献
Vene,J. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 1813 - 1817
反应条件
1: HNO3+H2SO4 / <0 / man verseift die Acetverbindungen mit verd.Salzsaeure
2: zinc; water
View Scheme
参考文献
Noelting; Braun; Thesmar
Chemische Berichte, 1901 , vol. 34, p. 2255
反应条件
1: HNO3, H2SO4
2: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, aq. CuSO4
3: H2SO4
4: H2SO4, aq. NaNO2
5: aq. NH3, aq. FeSO4 / Heating
6: aq. H2SO4, aq. NaNO2
View Scheme
参考文献
Vene,J. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 1813 - 1817
反应条件
1: HNO3+H2SO4 / <0 / man verseift die Acetverbindungen mit verd.Salzsaeure
2: tin; hydrochloric acid
View Scheme
参考文献
Noelting; Braun; Thesmar
Chemische Berichte, 1901 , vol. 34, p. 2255
反应条件
1: HNO3, H2SO4
2: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, aq. CuSO4
3: H2SO4
4: H2SO4, aq. NaNO2
5: H2SO4 / Heating
6: SnCl2, aq. HCl, AcOH
7: aq. NaNO2, aq. H2SO4
8: aq. NaOH
View Scheme
参考文献
Vene,J. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 1813 - 1817
反应条件
1: HNO3, H2SO4
2: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, aq. CuSO4
3: H2SO4
4: H2SO4, aq. NaNO2
5: H2SO4 / Heating
6: SnCl2, aq. HCl, AcOH
View Scheme
参考文献
Vene,J. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 1813 - 1817
反应条件
1: HNO3, H2SO4
2: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, aq. CuSO4
3: H2SO4
4: H2SO4, aq. NaNO2
5: H2SO4 / Heating
6: SnCl2, aq. HCl, AcOH
7: aq. NaNO2, aq. H2SO4
View Scheme
参考文献
Vene,J. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 1813 - 1817
