N-(2,3-二甲基苯基)乙酰胺合成路线 （共 30 条）
反应条件
triethylamine in dichloromethane T=0 - 20°C;
参考文献
Bayer Corporation
Patent: US6353006 B1, 2002 ;
Location in patent: Page column 28 ;
US 6353006 B1
反应条件
in chloroform T=20°C; 2 h;
参考文献
Havlik, Martin; Kral, Vladimir; Kaplanek, Robert; Dolensky, Bohumil
Organic Letters, 2008 , vol. 10, # 21 p. 4767 - 4769
反应条件
dihydrogen peroxide in water T=25°C; 8 h; Green chemistry;
参考文献
Sun, Xi; Wang, Min; Li, Pinhua; Zhang, Xiuli; Wang, Lei
Green Chemistry, 2013 , vol. 15, # 12 p. 3289 - 3294
参考文献
Toehl
Chemische Berichte, 1885 , vol. 18, p. 2562
Full Text Show Details
Noelting; Forel
Chemische Berichte, 1885 , vol. 18, p. 2677,2681
反应条件
1: HNO3, H2SO4 2: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, aq. CuSO4 3: H2SO4 4: H2SO4, aq. NaNO2 5: H2SO4 / Heating 6: SnCl2, aq. HCl, AcOH 7: aq. NaNO2, aq. H2SO4 8: aq. NaOH 9: aq. NaOH View Scheme
参考文献
Vene,J. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 1813 - 1817
反应条件
1: HNO3, H2SO4 2: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, aq. CuSO4 3: H2SO4 4: H2SO4, aq. NaNO2 5: aq. NH3, aq. FeSO4 / Heating View Scheme
参考文献
Vene,J. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 1813 - 1817
反应条件
1: HNO3+H2SO4 / <0 / man verseift die Acetverbindungen mit verd.Salzsaeure 2: zinc; water / in der Siedehitze View Scheme
参考文献
Noelting; Braun; Thesmar
Chemische Berichte, 1901 , vol. 34, p. 2255
反应条件
1: NBS, (PhCO)2O2 / CCl4 2: aq. H2SO4 View Scheme
参考文献
Kleinschmidt; Braeuniger
Die Pharmazie, 1969 , vol. 24, # 2 p. 87 - 94
反应条件
sulfuric acid; nitric acid; acetic acid T=15 - 16°C; 2 h;
参考文献
Helvetica Chimica Acta, , vol. 63, # 2 p. 385 - 394
反应条件
sulfuric acid; nitric acid T=0°C; 1 h;
参考文献
Organic Letters, , vol. 10, # 21 p. 4767 - 4769
