1,1,1,3-四氯庚烷合成路线 (共 15 条)
反应条件
[ReCl3(MeCN)(PPh3)2] in acetonitrile
2 h; Heating;
参考文献
Ivanov; Maksimov; Tomilova; Zefirov
Russian Chemical Bulletin, 2009 , vol. 58, # 11 p. 2393 - 2396
Izv. Akad. Nauk, Ser. Khim., 2009 , # 11 p. 2316 - 2319
反应条件
carbon monoxide; [(.eta.(5)-cyclopentadienyl)Mo(CO)3]2
T=91°C; P=147102 Torr;
参考文献
Susuki,T.; Tsuji,J.
Tetrahedron Letters, 1968 , p. 913 - 915
反应条件
dichlorotris(triphenylphosphine)ruthenium(II) in benzene
T=140°C; 36 h;
参考文献
Kamigata, Nobumasa; Sawada, Hideo; Suzuki, Norihiro; Kobayashi, Michio
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 199 - 204
反应条件
[(.eta.(5)-cyclopentadienyl)Mo(CO)3]2
T=91°C; P=147102 Torr;
参考文献
Susuki,T.; Tsuji,J.
Tetrahedron Letters, 1968 , p. 913 - 915
反应条件
chlorine in tetrachloromethane
T=25°C; Irradiation;
参考文献
Burton,T.; Bruylants,A.
Bulletin des Societes Chimiques Belges, 1972 , vol. 81, p. 639 - 642
反应条件
2,2'-azo-bisisobutyronitrile in tetrachloromethane
Yields of byproduct given;
参考文献
Degueil-Castaing, M.; Jeso, B. De; Kraus, G. A.; Landgrebe, K.; Maillard, B.
Tetrahedron Letters, 1986 , vol. 27, # 49 p. 5927 - 5930
反应条件
nano-Fe3O4; Titanium(IV) oxide in N,N-dimethyl-formamide
24 h; Ambient temperatureIrradiation;
参考文献
Mitani, Michiharu; Kiriyama, Takuya; Kuratate, Tomoaki
Journal of Organic Chemistry, 1994 , vol. 59, # 6 p. 1279 - 1282
反应条件
2,2'-azo-bisisobutyronitrile
Yield given;
参考文献
Degueil-Castaing, M.; Jeso, B. De; Kraus, G. A.; Landgrebe, K.; Maillard, B.
Tetrahedron Letters, 1986 , vol. 27, # 49 p. 5927 - 5930
反应条件
tetrachloromethane; Cr(acetylacetone)3
T=170°C; 6 h; Autoclave;
参考文献
Khusnutdinov; Schadneva; Oshnyakova; Dzhemilev
Petroleum Chemistry, 2009 , vol. 49, # 4 p. 331 - 338
反应条件
triethyl borane; oxygen; ytterbium(III) triflate in tetrahydrofuran; dichloromethane
T=20°C; Product distributionKinetics; Further Variations:SolventsReagents;
参考文献
Feng, Hao; Kavrakova, Ivanka K.; Pratt, Derek A.; Tellinghuisen, Joel; Porter, Ned A.
Journal of Organic Chemistry, 2002 , vol. 67, # 17 p. 6050 - 6054