反应条件
1: 99 percent / 1.) magnesium, 2-bromopropane / tetrahydrofuran / 1.) 30 min, reflux, 2.) 0 deg C, room temperature, 3 h 2: 1.) sodium hydride, n-butyllithium, 3.) 60percent H2SO4 / 1.) THF, 0 deg C, 30 min, 2.) heptane, room temperature, 1 h, 3.) reflux, 28 h View Scheme
参考文献
Baretz,B.H.; Turro,N.J.
Journal of the American Chemical Society, 1983 , vol. 105, p. 1309
