苄基-2-乙酰胺基-2-脱氧-Alpha-D-吡喃葡萄糖苷合成路线 （共 22 条）
反应条件
acetyl chloride T=20 - 50°C; 6 h; Inert atmosphere;
参考文献
Yamaguchi, Takao; Blazquez, Blas; Hesek, Dusan; Lee, Mijoon; Llarrull, Leticia I.; Boggess, Bill; Oliver, Allen G.; Fisher, Jed F.; Mobashery, Shahriar
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 3 p. 238 - 242
反应条件
hydrogenchloride T=85°C; 2 h; Title compound not separated from byproducts;
参考文献
, vol. 1986, # 1 p. 37 - 45
反应条件
toluene-4-sulfonic acid in toluene 3 h; Reflux;
参考文献
Babic, Andrej; Pecar, Slavko
Tetrahedron Asymmetry, 2008 , vol. 19, # 19 p. 2265 - 2271
反应条件
in N,N-dimethyl-formamide T=20°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 42, # 43 p. 7567 - 7570
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide T=20°C; 0.166667 h; optical yield given as percent de;
参考文献
Organic Letters, , vol. 10, # 16 p. 3461 - 3463
反应条件
1.1: Na / methanol 1.2: 98 percent / 20 °C 2.1: 63 percent / PTSA / benzene / 12 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 48, # 25 p. 4403 - 4405
反应条件
1: 77 percent / HCl / 100 °C 2: 1.) H2 / 1.) Pd-black / 1.) THF-MeOH; 2.) THF-MeOH, roomtemp., 1 h View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, # 5 p. 1419 - 1424
反应条件
1: 77 percent / HCl / 100 °C 2: 1.) H2 / 1.) Pd-black / 1.) THF-MeOH; 2.) THF-MeOH, roomtemp., 1 h View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, # 5 p. 1419 - 1424
反应条件
hydrogen; palladium 1.) THF-MeOH; 2.) THF-MeOH, roomtemp., 1 h; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, # 5 p. 1419 - 1424
