2,6-二甲基-4-亚硝基苯酚合成路线 （共 10 条）
反应条件
acetic acid; sodium nitrite in ethanol
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
反应条件
acetic acid; sodium nitrite in ethanol Nitration; nitrosation; 0.166667 h;
参考文献
Tetrahedron, , vol. 55, # 49 p. 14111 - 14122
反应条件
1: 69 percent / PtO2, H2 / acetic acid / 2 h / Ambient temperature 2: 65 percent / Pb(OAc)4 / ethyl acetate / Ambient temperature 3: 41 percent / H2O / acetone / 5 h / Heating View Scheme
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
反应条件
platinum(IV) oxide; hydrogen in acetic acid 2 h; Ambient temperature;
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
参考文献
Rowe; Bannister; Storey
Journal of the Society of Chemical Industry, London, 1931 , vol. 50, p. 79 T
反应条件
sulfuric acid in ethylene glycol
T=105°C;
参考文献
Ruzicka,E. et al.
Collection of Czechoslovak Chemical Communications, 1972 , vol. 37, p. 1905 - 1907
反应条件
sulfuric acid
T=40°C; 6 h;
参考文献
Ruzicka,E. et al.
Collection of Czechoslovak Chemical Communications, 1972 , vol. 37, p. 1905 - 1907
反应条件
sulfuric acid in ethylene glycol
T=105°C;
参考文献
Ruzicka,E. et al.
Collection of Czechoslovak Chemical Communications, 1972 , vol. 37, p. 1905 - 1907
反应条件
1: 69 percent / PtO2, H2 / acetic acid / 2 h / Ambient temperature
2: 65 percent / Pb(OAc)4 / ethyl acetate / Ambient temperature
View Scheme
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
反应条件
1: 69 percent / PtO2, H2 / acetic acid / 2 h / Ambient temperature
2: 65 percent / Pb(OAc)4 / ethyl acetate / Ambient temperature
3: 49 percent / CH2Cl2 / 72 h / Ambient temperature
View Scheme
参考文献
Fernando; Calder; Ham
Journal of Medicinal Chemistry, 1980 , vol. 23, # 11 p. 1153 - 1158
