反应条件
1: iodobenzene With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
Suzuki coupling; 0.25 h;
2: 4-((5,5-dimethyl-1,3,2-dioxaborinan-2-yl)ethynyl)pyridyl With caesium carbonate in N,N-dimethyl-formamide
T=50°C; Suzuki coupling; 72 h;
参考文献
Kaae, Birgitte H.; Harpsoe, Kasper; Kvist, Trine; Mathiesen, Jesper M.; Molck, Christina; Gloriam, David; Jimenez, Hermogenes N.; Uberti, Michelle A.; Nielsen, Soren M.; Nielsen, Birgitte; Braeuner-Osborne, Hans; Sauerberg, Per; Clausen, Rasmus P.; Madsen, Ulf
ChemMedChem, 2012 , vol. 7, # 3 p. 440 - 451