1-叔丁基-4-亚甲基环己烷合成路线 （共 50 条）
反应条件
sulfuric acid in cyclohexane
0.5 h; Heating;
参考文献
Bates, Tim F.; Dandekar, Sushama A.; Longlet, Jon J.; Thomas, Ruthanne D.
Journal of Organometallic Chemistry, 2001 , vol. 625, # 1 p. 13 - 22
反应条件
quinoline; copper
T=240 - 250°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Picard, Philippe; Moulines, Jean; Lecoustre, Max
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 65 - 70
反应条件
(i) nBuLi, THF, (ii) /BRN= 507309/; Multistep reaction;
参考文献
Corey,E.J.; Kwiatkowski,G.T.
Journal of the American Chemical Society, 1966 , vol. 88, p. 5654 - 5656
反应条件
(i) nBuLi, Ph3CH, THF, (ii) Al-Hg, AcOH; Multistep reaction;
参考文献
Johnson,C.R.; Kirchhoff,R.A.
Journal of the American Chemical Society, 1979 , vol. 101, p. 3602 - 3607
反应条件
in diethyl ether
20 h; from -15 degC to 20 degC;
参考文献
Kauffmann, Thomas; Koenig, Rolf; Pahde, Claudia; Tannert, Annegret
Tetrahedron Letters, 1981 , vol. 22, # 50 p. 5031 - 5034
反应条件
(thermolysis) in benzene
T=116.4 - 129.9°C; Kinetics;
参考文献
King,J.F.; Coppen,M.J.
Canadian Journal of Chemistry, 1971 , vol. 49, p. 3714 - 3723
反应条件
(thermolysis) in benzene
T=116.4 - 129.9°C; Kinetics;
参考文献
King,J.F.; Coppen,M.J.
Canadian Journal of Chemistry, 1971 , vol. 49, p. 3714 - 3723
参考文献
Sekiguchi,A.; Auclo,W.
Chemistry Letters, 1978 , p. 1385 - 1386
反应条件
n-butyllithium
1.) THF, hexane, -78 deg C, 45 min, 2.) THF, hexane, -78 deg C, 60 min; Yield given. Multistep reaction;
参考文献
Hanessian, Stephen; Bennani, Youssef L.; Leblanc, Yves
Heterocycles, 1993 , vol. 35, # 2 p. 1411 - 1424
反应条件
1: 50percent aq. KOH
2: quinoline, Cu / 240 - 250 °C
View Scheme
参考文献
Picard, Philippe; Moulines, Jean; Lecoustre, Max
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 65 - 70
