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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
13259-28-4
合成路线
（共 8 条）
13259-28-4
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
反应条件
1: pyridine / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 2: SAM II lipase; sodium hydroxide / pentane; tert-butyl methyl ether; aq. phosphate buffer / 20 °C / pH 7 / |Inert atmosphere; |Enzymatic reaction 3: acetic acid; dihydrogen peroxide / water / 24 h / 0 °C View Scheme
参考文献
Lentsch, Christoph; Fuerst, Rita; Mulzer, Johann; Rinner, Uwe
European Journal of Organic Chemistry, 2014 , vol. 2014, # 5 p. 919 - 923
13259-28-4
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
26054-46-6
前列腺素中间体
+
103618-27-5
反应条件
oxygen monooxygenase from Pseudomonas putida NCIMB 10007, Pseudomonas sp. NCIMB 9872 (DH 9872); Title compound not separated from byproducts;
参考文献
Grogan, Gideon; Roberts, Stanley M.; Willetts, Andrew J.
Journal of the Chemical Society, Chemical Communications, 1993 , # 8 p. 699 - 701
13259-28-4
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
反应条件
1: pyridine / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 2: SAM II lipase; sodium hydroxide / pentane; tert-butyl methyl ether; aq. phosphate buffer / 20 °C / pH 7 / |Inert atmosphere; |Enzymatic reaction 3: acetic acid; dihydrogen peroxide / water / 24 h / 0 °C View Scheme
参考文献
Lentsch, Christoph; Fuerst, Rita; Mulzer, Johann; Rinner, Uwe
European Journal of Organic Chemistry, 2014 , vol. 2014, # 5 p. 919 - 923
13259-28-4
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
26054-46-6
前列腺素中间体
+
103618-27-5
反应条件
oxygen monooxygenase from Pseudomonas putida NCIMB 10007, Pseudomonas sp. NCIMB 9872 (DH 9872); Title compound not separated from byproducts;
参考文献
Grogan, Gideon; Roberts, Stanley M.; Willetts, Andrew J.
Journal of the Chemical Society, Chemical Communications, 1993 , # 8 p. 699 - 701
108-24-7
乙酸酐
+
13259-28-4
→
反应条件
1521-45-5
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane
参考文献
Klempier, Norbert; Geymayer, Paul; Stadler, Peter; Faber, Kurt; Griengl, Herfried
Tetrahedron: Asymmetry, 1990 , vol. 1, # 2 p. 111 - 118
13259-28-4
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
反应条件
1: pyridine / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 2: SAM II lipase; sodium hydroxide / pentane; tert-butyl methyl ether; aq. phosphate buffer / 20 °C / pH 7 / |Inert atmosphere; |Enzymatic reaction 3: acetic acid; dihydrogen peroxide / water / 24 h / 0 °C View Scheme
参考文献
Lentsch, Christoph; Fuerst, Rita; Mulzer, Johann; Rinner, Uwe
European Journal of Organic Chemistry, 2014 , vol. 2014, # 5 p. 919 - 923
13259-28-4
→
反应条件
34638-25-0
3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮
+
26054-46-6
前列腺素中间体
+
103618-27-5
反应条件
oxygen monooxygenase from Pseudomonas putida NCIMB 10007, Pseudomonas sp. NCIMB 9872 (DH 9872); Title compound not separated from byproducts;
参考文献
Grogan, Gideon; Roberts, Stanley M.; Willetts, Andrew J.
Journal of the Chemical Society, Chemical Communications, 1993 , # 8 p. 699 - 701
13259-28-4
→
反应条件
13173-09-6
双环[3,2,0]庚-2-烯-6-酮
反应条件
oxidizing under Collins condition;
参考文献
Dawson, Michael J.; Lawrence, Gordon C.; Lilley, Gerald; Todd, Martin; Noble, David; at al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2119 - 2125
