二(4-甲基苄基)-硫醚合成路线 （共 17 条）
反应条件
di-tert-butyl peroxide; dicobalt octacarbonyl in benzene T=185°C; P=44080 Torr; in N2-atm.;
参考文献
Antebi, Shlomo; Alper, Howard
Tetrahedron Letters, 1985 , vol. 26, # 22 p. 2609 - 2612
反应条件
1: p-methylbenzyl bromide With thiourea in methanol Inert atmosphereReflux; 2: With sodium hydroxide in methanol Inert atmosphereReflux; 3: p-methylbenzyl bromide in methanol T=20°C; Inert atmosphereReflux;
参考文献
Eccles, Kevin S.; Elcoate, Curtis J.; Lawrence, Simon E.; Maguire, Anita R.
Arkivoc, 2010 , vol. 2010, # 9 p. 216 - 228
反应条件
dicobalt octacarbonyl in benzene T=185°C; P=44080 Torr; in CO-atm.;
参考文献
Antebi, Shlomo; Alper, Howard
Tetrahedron Letters, 1985 , vol. 26, # 22 p. 2609 - 2612
反应条件
tetra(n-butyl)ammonium hydrogen sulphate in water; ethyl acetate
参考文献
Ciba-Geigy Corporation
Patent: US5247113 A1, 1993 ;
反应条件
dicobalt octacarbonyl in benzene T=180°C; P=56886.3 - 67229.2 Torr; stainless steel autoclave;
参考文献
Antebi, Shlomo; Alper, Howard
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2010 - 2012
反应条件
2,4,6-trichloro-1,3,5-triazine in 1,4-dioxane 12 h; Heating;
参考文献
Olah, George A.; Fung, Alexander P.; Gupta, B.G. Balaram; Narang, Subhash C.
Synthesis, 1980 , # 3 p. 221
反应条件
tetrafluoroboric acid; dodecacarbonyltriiron in benzene 1.) RT, 4 h; 2.) 60 deg C, product ratio dependence to amount of Fe3(CO)12;
参考文献
Alper, Howard; Sibtain, Fazle
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 225 - 230
参考文献
Oae, Shigeru; Yamada, Norihiro; Fujimori, Ken; Kikuchi, Osamu
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 1 p. 248 - 256
反应条件
tetrafluoroboric acid; dodecacarbonyltriiron; sodium dodecylbenzenesulfonate in benzene 1.) RT, 4 h; 2.) 60 deg C;
参考文献
Alper, Howard; Sibtain, Fazle
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 225 - 230
反应条件
sodium hydroxide; dicobalt octacarbonyl; tetra(n-butyl)ammonium hydrogensulfate in water; benzene T=60°C; 16 h;
参考文献
Alper, Howard; Sibtain, Fazle; Heveling, Josef
Tetrahedron Letters, 1983 , vol. 24, # 48 p. 5329 - 5332
