反应条件
1: 1.) BuLi, 3.) LAH / 1.) THF/hexane, -78 deg C, 30 min, 2.) THF/hexane, -78 -> -10 deg C, 3.) THF, RT, 6 h 2: 96 percent / gaseous HBr / diethyl ether / 1 h / 0 °C View Scheme
参考文献
Heffner; Joullie
Synthetic Communications, 1991 , vol. 21, # 8-9 p. 1055 - 1069
