1,6-脱水-β-D-葡萄糖-2,3,4-三邻醋酸合成路线 (共 48 条)
反应条件
silica-supported perchloric acid in acetonitrile T=70°C; 0.0333333 h; Inert atmosphere;
参考文献
Chun, Yuexing; Yan, Shiqiang; Li, Xiangpeng; Ding, Ning; Zhang, Wei; Wang, Peng; Li, Ming; Li, Yingxia
Tetrahedron Letters, 2011 , vol. 52, # 46 p. 6196 - 6198
反应条件
scandium tris(trifluoromethanesulfonate) T=20°C; 0.2 h;
参考文献
Lee, Jinq-Chyi; Tai, Cheng-An; Hung, Shang-Cheng
Tetrahedron Letters, 2002 , vol. 43, # 5 p. 851 - 855
反应条件
iron(III) chloride in dichloromethane T=40°C; 0.333333 h;
参考文献
Miranda, Pedro O.; Brouard, Ignacio; Padron, Juan I.; Bermejo, Jaime
Tetrahedron Letters, 2003 , vol. 44, # 20 p. 3931 - 3934
反应条件
tin(IV) chloride in 1,2-dichloro-ethane T=25°C; 12 h; variation of Lewis acids; Product distribution;
参考文献
Rao, Mothe Vaman; Nagarajan, Madhavarao
Carbohydrate Research, 1987 , vol. 162, p. 141 - 144
反应条件
tris(trifluoro acetyloxy)borane in trifluoroacetic acid 0.0833333 h; Ambient temperature;
参考文献
Tewson, Timothy J.
Journal of Organic Chemistry, 1983 , vol. 48, # 20 p. 3507 - 3510
反应条件
iron(III) chloride in dichloromethane T=40°C; 3 h;
参考文献
Miranda, Pedro O.; Brouard, Ignacio; Padron, Juan I.; Bermejo, Jaime
Tetrahedron Letters, 2003 , vol. 44, # 20 p. 3931 - 3934
反应条件
1: 1,2,3,4-tetra-O-acetyl-6-O-p-tolylsulfonyl-α,β-D-glucopyranose With aluminum oxide T=110°C; 0.116667 h; microwave irradiation; 2: acetic anhydride With potassium acetate T=100°C; 0.333333 h;
参考文献
Bailliez, Vincent; De Figueiredo, Renata M.; Olesker, Alain; Cleophax, Jeannine
Synthesis, 2003 , # 7 p. 1015 - 1017
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane Ambient temperature;
参考文献
Lafont, Dominique; Boullanger, Paul; Cadas, Olivier; Descotes, Gerard
Synthesis, 1989 , # 3 p. 191 - 194
反应条件
Ph3C+ClO4- in dichloromethane T=20°C; 336 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 5 p. 1056 - 1061
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 5 p. 1170 - 1177
反应条件
hydrogenchloride; zinc
参考文献
Journal of the American Chemical Society, , vol. 69, p. 249