3,3’,4,4’-四氨基二苯砜(TADS)合成路线 (共 5 条)
反应条件
hydrazine hydrate; nickel in tetrahydrofuran; ethanol 3 h; Heating;
参考文献
Abuzar; Sharma; Visen; Gupta; Katiyar
Arzneimittel-Forschung/Drug Research, 1986 , vol. 36, # 3 p. 416 - 419
反应条件
1: fuming sulfuric acid; hydrogen chloride / Edukt 4:SO3 2: AlCl3 3: H2SO4; HNO3 4: alcohol; ammonia / 150 °C 5: tin dichloride View Scheme
参考文献
Ullmann; Korselt
Chemische Berichte, 1907 , vol. 40, p. 645
反应条件
water; nitric acid und anschliessend mit SnCl2 und wss. HCl;
参考文献
Matsukawa et al.
Yakugaku Zasshi, 1950 , vol. 70, p. 77,79
Chem.Abstr., 1950 , p. 5322
反应条件
1: H2SO4; HNO3 2: alcohol; ammonia / 150 °C 3: tin dichloride View Scheme
参考文献
Ullmann; Korselt
Chemische Berichte, 1907 , vol. 40, p. 645
反应条件
1: AlCl3 2: H2SO4; HNO3 3: alcohol; ammonia / 150 °C 4: tin dichloride View Scheme
参考文献
Ullmann; Korselt
Chemische Berichte, 1907 , vol. 40, p. 645