(2-氨基苯基)(苯基)甲醇合成路线 (共 39 条)
反应条件
sodium tetrahydroborate in ethanol 2 h; Heating;
参考文献
Martinez-Viturro, Carlos M.; Dominguez, Domingo
Tetrahedron Letters, 2007 , vol. 48, # 6 p. 1023 - 1026
反应条件
tetra-N-butylammonium borohydride; Ni(2,2'-bipyridine) in N,N-dimethyl-formamide T=20°C; Electrochemical reaction;
参考文献
Budnikova; Keshner; Kargin
Russian Journal of General Chemistry, 2001 , vol. 71, # 3 p. 453 - 456
反应条件
potassium hydroxide in methanol 1.5 h; Heating;
参考文献
Fleming, Ian; Loreto, Maria Antonietta; Wallace, Ian H.M.; Michael, Joseph P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 349 - 360
反应条件
sodium tetrahydroborate; NiII chloride hexahydrate in ethanol T=0°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 73, # 21 p. 8608 - 8611
反应条件
1: D2O, KOH 2: 1.) n-butyl-lithium / 1.) hexane, THF, 4 h, -78 deg C; 2.) THF, 2 h, -78 deg C 3: 89 percent / 1.2M aq. potassium hydroxide / methanol / 1.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 349 - 360
反应条件
1: diethyl ether / Erhitzen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit CrO3 in Essigsaeure 2: Raney nickel; ethyl acetate / Hydrogenation 3: chloroform; bromine 4: sodium-amalgam; aqueous ethanol 5: palladium/calcium carbonate; methanol. KOH-solution / Hydrogenation View Scheme
参考文献
Helvetica Chimica Acta, , vol. 24, p. 703,714
反应条件
1: 1.) n-butyl-lithium / 1.) hexane, THF, 4 h, -78 deg C; 2.) THF, 2 h, -78 deg C 2: 89 percent / 1.2M aq. potassium hydroxide / methanol / 1.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 349 - 360
反应条件
1: 1.) n-butyl-lithium / 1.) hexane, THF, -110 deg C, 3 h; 2.) THF, hexane, -105 deg C, 1 h, 3 h at -78 deg C 2: 89 percent / 1.2M aq. potassium hydroxide / methanol / 1.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 349 - 360
反应条件
1: in tetrahydrofuran; diethyl ether 2: With water; ammonium chloride in tetrahydrofuran; diethyl ether
参考文献
Chemical Communications, , vol. 47, # 33 p. 9513 - 9515
反应条件
1: Raney nickel; ethyl acetate / Hydrogenation 2: chloroform; bromine 3: sodium-amalgam; aqueous ethanol 4: palladium/calcium carbonate; methanol. KOH-solution / Hydrogenation View Scheme
参考文献
Helvetica Chimica Acta, , vol. 24, p. 703,714