oxygen; lithium chloride; copper dichloride; [Pd2(MeCOCHCOCHCOPh){(S)-Ph-BINAP}X2] in tetrahydrofuran; water
T=25°C; Oxidation; P=760 Torr; Title compound not separated from byproducts;
参考文献
El-Qisairi, Arab; Hamed, Othman; Henry, Patrick M.
Journal of Organic Chemistry, 1998 , vol. 63, # 9 p. 2790 - 2791
1: pyridine / 10 h / 100 °C / other reagents, other time and temp.
2: Ambient temperature
3: water, NaOH / 52 h / Ambient temperature; Lipase PS "Amano", phosphate buffer (pH 7)
View Scheme
参考文献
Bevinakatti; Banerji
Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 5372 - 5375
water in various solvent(s)
T=25°C; 144 h; native lipase B from Candida antarctica; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bermudez, Jose L.; Del Campo, Carmen; Salazar, Loreto; Llama, Emilio F.; Sinisterra, Jose V.
Tetrahedron Asymmetry, 1996 , vol. 7, # 9 p. 2485 - 2488
