1-溴-4-[(1E)-2-硝基-1-丙烯-1-基]苯合成路线 (共 7 条)
反应条件
phenolformaldehyde-based ethylenediamine-modified polymer T=90°C; Henry reaction; 6 h;
参考文献
Yan, Shaoyu; Gao, Yuan; Xing, Rong; Shen, Yali; Liu, Yueming; Wu, Peng; Wu, Haihong
Tetrahedron, 2008 , vol. 64, # 27 p. 6294 - 6299
反应条件
ammonium acetate in acetic acid T=50°C; P=7500600 Torr; 3 h;
参考文献
Agafonov, N. E.; Sedishev, I. P.; Dudin, A. V.; Kutin, A. A.; Stashina, G. A.; Zhulin, V. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 2.2 p. 366 - 372
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 2 p. 426 - 433
反应条件
(E,Z)-crotononitrile; ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride; piperidinium acetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene 8 h; Inert atmosphereReflux;
参考文献
Hall, Michael I.; Pridmore, Simon J.; Williams, Jonathan M. J.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 13 p. 1975 - 1978
反应条件
tin(ll) chloride in ethyl acetate 5 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Kabalka, George W.; Goudgaon, Naganna M.
Synthetic Communications, 1988 , vol. 18, # 7 p. 693 - 698
反应条件
chromium dichloride in tetrahydrofuran; hydrogenchloride 4 h; Heating;
参考文献
Varma, Rajender S.; Varma, Manju; Kabalka, George W.
Tetrahedron Letters, 1985 , vol. 26, # 32 p. 3777 - 3778
反应条件
ammonium formate; palladium on activated charcoal in tetrahydrofuran; methanol 2.5 h; Ambient temperature;
参考文献
Kabalka, George W.; Pace, R. David; Wadgaonkar, P.P.
Synthetic Communications, 1990 , vol. 20, # 16 p. 2453 - 2458
反应条件
ammonium formate; palladium on activated charcoal in tetrahydrofuran; methanol 2.5 h; Ambient temperature;
参考文献
Kabalka, George W.; Pace, R. David; Wadgaonkar, P.P.
Synthetic Communications, 1990 , vol. 20, # 16 p. 2453 - 2458