1,4-双(三甲基甲硅烷基)苯合成路线 （共 36 条）
反应条件
silver tetrafluoroborate; iodine cloride in tetrahydrofuran; methanol T=-35°C; 1 h;
参考文献
Jacob; Chen; Stec
Synthesis, 1993 , # 6 p. 611 - 614
反应条件
potassium in ethylene glycol dimethyl ether 1.) -20 deg C -> 10 deg C, 2.) room temperature, 1 h;
参考文献
Bock,H.; Kaim,W.
Journal of the American Chemical Society, 1980 , vol. 102, p. 4429
反应条件
1: nitric acid; acetic anhydride / 1.5 h / Reflux 2: palladium 10 on activated carbon; hydrogen / toluene / 760.05 Torr View Scheme
参考文献
Lothian, Aileen P.; Ramsden, Christopher A.; Shaw, Maxine M.; Smith, Rachel G.
Tetrahedron, 2011 , vol. 67, # 15 p. 2788 - 2793
反应条件
1: BCl3 / CH2Cl2 / 10 h / 25 °C
2: Br2 / 16 h / 25 °C
View Scheme
参考文献
Hupe, Eike; Calaza, M. Isabel; Knochel, Paul
Chemical Communications, 2002 , # 13 p. 1390 - 1391
反应条件
nitric acid; acetic anhydride
1.5 h; Reflux;
参考文献
Lothian, Aileen P.; Ramsden, Christopher A.; Shaw, Maxine M.; Smith, Rachel G.
Tetrahedron, 2011 , vol. 67, # 15 p. 2788 - 2793
参考文献
Deans; Eaborn
Journal of the Chemical Society, 1957 , p. 498
