1,4-双(三甲基甲硅烷基)苯合成路线 （共 36 条）
反应条件
1: nitric acid; acetic anhydride / 1.5 h / Reflux 2: XeF2 / hexafluorobenzene / 1 h / 20 °C / Pyrex.(R). vessel View Scheme
参考文献
Lothian, Aileen P.; Ramsden, Christopher A.; Shaw, Maxine M.; Smith, Rachel G.
Tetrahedron, 2011 , vol. 67, # 15 p. 2788 - 2793
反应条件
sulfur trioxide in tetrachloromethane Heating;
参考文献
Bott,R.W. et al.
Journal of Organometallic Chemistry, 1965 , vol. 3, p. 442 - 447
参考文献
Bourgeois,P.; Calas,R.
Journal of Organometallic Chemistry, 1975 , vol. 84, p. 165 - 175
反应条件
in tetrachloromethane
参考文献
Bott,R.W. et al.
Journal of Organometallic Chemistry, 1965 , vol. 3, p. 442 - 447
Full Text View citing articles Show Details
Gmelin Handbook: S: SVol.3, 3.1.7.8.2, page 320 - 322
反应条件
aluminium trichloride in carbon disulfide
参考文献
Dey,K. et al.
Organometallics in Chemical Synthesis, 1970 , vol. 1, p. 151 - 160
反应条件
1.1: BCl3 / CH2Cl2 / 10 h / 25 °C 2.1: Br2 / 16 h / 25 °C 3.1: i-Pr2Zn / diethyl ether / 2 h / 25 °C 3.2: CuCN*2LiCl / tetrahydrofuran / 0.17 h / -30 °C 3.3: 62 percent / tetrahydrofuran / 20 °C View Scheme
参考文献
Hupe, Eike; Calaza, M. Isabel; Knochel, Paul
Chemical Communications, 2002 , # 13 p. 1390 - 1391
反应条件
trifluoroacetic acid in dichloromethane 48 h; Ambient temperature;
参考文献
Kuehl; Bolz; Zhdankin
Synthesis, 1995 , # 3 p. 312 - 316
反应条件
silver tetrafluoroborate; iodine cloride in methanol T=0°C; 1 h;
参考文献
Jacob; Chen; Stec
Synthesis, 1993 , # 6 p. 611 - 614
反应条件
1.1: BCl3 / CH2Cl2 / 10 h / 25 °C 2.1: Br2 / 16 h / 25 °C 3.1: i-Pr2Zn / diethyl ether / 2 h / 25 °C 3.2: CuCN*2LiCl / tetrahydrofuran / 0.17 h / -30 °C 3.3: 68 percent / tetrahydrofuran / 20 °C View Scheme
参考文献
Hupe, Eike; Calaza, M. Isabel; Knochel, Paul
Chemical Communications, 2002 , # 13 p. 1390 - 1391
反应条件
1: BCl3 / CH2Cl2 / 16 h / 25 °C 2: ICl / CH2Cl2 / 16 h / 25 °C 3: 54 percent / iPrZn / 2 h / 25 °C View Scheme
参考文献
Hupe, Eike; Calaza, M. Isabel; Knochel, Paul
Chemical Communications, 2002 , # 13 p. 1390 - 1391
