3,3,8,8-四乙基-4,7-二氧杂-3,8-二硅杂癸烷合成路线 （共 6 条）
反应条件
air; hydrido(triphenylphosphine)copper(I) hexamer in benzene 5 h; Ambient temperature;
参考文献
Lorenz, Catrin; Schubert, Ulrich
Chemische Berichte, 1995 , vol. 128, # 12 p. 1267 - 1270
参考文献
Diekman,J. et al.
Journal of Organic Chemistry, 1968 , vol. 33, # 6 p. 2271 - 2284
反应条件
[RhCl(PPh3)2] in N,N-dimethyl acetamide; water T=20°C; 71 h;
参考文献
Chung; Ferguson; Robertson; Schlaf
Canadian Journal of Chemistry, 2001 , vol. 79, # 5-6 p. 949 - 957
反应条件
zinc(II) chloride T=120°C; 140 h;
参考文献
Frainnet,E.; Esclamadon,C.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1962 , vol. 254, p. 1814 - 1816
反应条件
nickel T=65°C; 2 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Mel'nitskii, I. A.; Kiladze, T. K.; Kantor, E. A.; Rakhmankulov, D. L.; Paushkin, Ya. M.
Doklady Chemistry, 1985 , vol. 280, p. 60 - 61
Dokl. Akad. Nauk SSSR Ser. Khim., 1985 , vol. 280, # 5 p. 1152 - 1154
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-78°C; 4.5 h;
参考文献
THE UNIVERSITY OF BRITISH COLUMBIA
Patent: WO2004/54957 A2, 2004 ;
Location in patent: Page 23-24 ;
