D-(-)-酒石酸二甲酯合成路线 (共 11 条)
反应条件
ruthenium trichloride; sodium periodate in ethyl acetate; acetonitrile 0.05 h;
参考文献
Shing, Tony K. M.; Tam, Eric K. W.; Tai, Vincent W.-F.; Chung, Ivan H. F.; Jiang, Qin
Chemistry--A European Journal, 1996 , vol. 2, # 1 p. 50 - 57
反应条件
di(n-butyl)tin oxide in methanol 12 h; Heating;
参考文献
Baumhof, Patrick; Mazitschek, Ralph; Giannis, Athanassios
Angewandte Chemie - International Edition, 2001 , vol. 40, # 19 p. 3672 - 3674
反应条件
dihydrogen peroxide; Kemp's acid derived iron(II) in acetonitrile T=25°C; 2 h;
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 47 p. 7975 - 7978
反应条件
hydrogenchloride ice bath;
参考文献
Bell, H. M.; Hudlicky, M.
Journal of Fluorine Chemistry, 1980 , vol. 15, p. 191 - 200
反应条件
in methanol; diethyl ether
参考文献
Helvetica Chimica Acta, , vol. 66, # 8 p. 2501 - 2511
反应条件
nitric acid 1.) water, 2 h reflux; 2.) methanol/ether; Yield given. Multistep reaction. Further byproducts given;
参考文献
Helvetica Chimica Acta, , vol. 64, # 2 p. 407 - 424
反应条件
toluene-4-sulfonic acid in dichloromethane 6 h; Reflux;
参考文献
Wang, Liping; Zhu, Weiming
Tetrahedron Letters, 2013 , vol. 54, # 49 p. 6729 - 6731
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane T=20°C; 12 h;
参考文献
Hernandez-Torres, Gloria; Carreno, M. Carmen; Urbano, Antonio; Colobert, Franacoise
Chemistry - A European Journal, 2011 , vol. 17, # 4 p. 1283 - 1293
反应条件
potassium iodide; silver(l) oxide in dichloromethane 15 h; Ambient temperature;
参考文献
Bouzide, Abderrahim; Sauve, Gilles
Tetrahedron Letters, 1997 , vol. 38, # 34 p. 5945 - 5948
反应条件
tetra-(n-butyl)ammonium iodide; sodium hydride in tetrahydrofuran
参考文献
Hernandez-Torres, Gloria; Carreno, M. Carmen; Urbano, Antonio; Colobert, Franacoise
Chemistry - A European Journal, 2011 , vol. 17, # 4 p. 1283 - 1293