(三甲基硅基)甲基氯化镁合成路线 (共 130 条)
反应条件
potassium carbonate; nickel 2.) MeOH; Yield given. Multistep reaction;
参考文献
Bamba, Makoto; Nishikawa, Toshio; Isobe, Minoru
Tetrahedron Letters, 1996 , vol. 37, # 45 p. 8199 - 8202
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether Ambient temperature;
参考文献
Sengupta, Saumitra; Leite, Magda; Raslan, Delio Soares; Quesnelle, Claude; Snieckus, Victor
Journal of Organic Chemistry, 1992 , vol. 57, # 15 p. 4066 - 4068
参考文献
Tamao,K. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 1958 - 1969
反应条件
phosphorus tribromide
参考文献
Seyferth
Journal of the American Chemical Society, 1958 , vol. 80, p. 1336
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether 10 h; Ambient temperature;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Okamoto, Yasuo; Kumada, Makoto
Tetrahedron Letters, 1981 , vol. 22, # 44 p. 4449 - 4452
参考文献
Tamao,K. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 1958 - 1969
反应条件
in tetrahydrofuran 20 h reflux;
参考文献
Seyferth
Journal of the American Chemical Society, 1957 , vol. 79, p. 5881
参考文献
Mironow; Pogonkina
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 182,183,185;engl.Ausg.S.161,162,163
反应条件
trichlorosilane in diethyl ether Heating;
参考文献
Whitmarsh, Chris K.; Interrante, Leonard V.
Journal of Organometallic Chemistry, 1991 , vol. 418, # 1 p. 69 - 77
反应条件
lithium aluminium tetrahydride; trichlorosilane 1.) ether, reflux, overnight; Multistep reaction;
参考文献
Whitmarsh, Chris K.; Interrante, Leonard V.
Journal of Organometallic Chemistry, 1991 , vol. 418, # 1 p. 69 - 77