1-甲氧基-1,2-丙二烯合成路线 （共 58 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide; tert-butyl alcohol in tetrahydrofuran T=20°C; Title compound not separated from byproducts;
参考文献
Chemistry - A European Journal, , vol. 10, # 21 p. 5493 - 5506
反应条件
platinum (II) chloride in tetrahydrofuran; water T=55°C; 16 h; Inert atmosphere;
参考文献
Bhuvaneswari, Sivakolundu; Jeganmohan, Masilamani; Cheng, Chien-Hong
Chemistry - An Asian Journal, 2010 , vol. 5, # 1 p. 141 - 146
反应条件
sodium hydrogencarbonate; copper dichloride; palladium dichloride T=10 - 13°C; 5 h;
参考文献
Trofimov, Boris A.; Mal'kina, Anastasiya G.; Kudyakova, Ravilya N.; Tarasova, Ol'ga A.; Nosyreva, Valentina V.; Afonin, Andrei V.
Mendeleev Communications, 2004 , vol. 14, # 2 p. 61 - 63
反应条件
sodium hydrogencarbonate; copper dichloride T=-5 - 22°C; 1 h;
参考文献
Trofimov, Boris A.; Mal'kina, Anastasiya G.; Kudyakova, Ravilya N.; Tarasova, Ol'ga A.; Nosyreva, Valentina V.; Afonin, Andrei V.
Mendeleev Communications, 2004 , vol. 14, # 2 p. 61 - 63
反应条件
sodium hydrogencarbonate; copper dichloride; palladium dichloride T=-5 - 22°C; 2 h; Product distribution; Further Variations:Temperatures;
参考文献
Trofimov, Boris A.; Mal'kina, Anastasiya G.; Kudyakova, Ravilya N.; Tarasova, Ol'ga A.; Nosyreva, Valentina V.; Afonin, Andrei V.
Mendeleev Communications, 2004 , vol. 14, # 2 p. 61 - 63
反应条件
copper(l) chloride in diethyl ether
参考文献
Meijer,J.; Vermeer,P.
Recueil des Travaux Chimiques des Pays-Bas, 1974 , vol. 93, p. 183
反应条件
copper(l) iodide; sodium cyanide; water; ammonium chloride 1.) Et2O, 20-30 deg C, 30 min, 2.) Et2O, 40 min; Yield given. Multistep reaction;
参考文献
Fleming, Ian; Morgan, Ian T.; Sarkar, Achintya K.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 17 p. 2749 - 2763
反应条件
tris(pentafluorophenyl)-borane in toluene under Ar, -78°C, 3 h;
参考文献
Asao, Naoki; Yamamoto, Yoshinori
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 5 p. 1071 - 1087
反应条件
n-butyllithium in tetrahydrofuran
1.) -23 deg C, 1 h, 2.) -20 deg C;
参考文献
Kucerovy, Andrew; Neuenschwander, Kent; Weinreb, Steven M.
Synthetic Communications, 1983 , vol. 13, # 11 p. 875 - 880
参考文献
Hoff,S. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1968 , vol. 87, p. 916 - 924
