1-叔丁基-3-氮杂环丁醇合成路线 （共 9 条）
反应条件
1: in isopropyl alcohol T=25°C; 2: With triethylamine in acetonitrile T=100°C; 24 h;
参考文献
WO2010/59393 A1, ;
Page/Page column 160 ;
WO 2010/059393 A1
反应条件
triethylamine in acetonitrile 16 h; Heating;
参考文献
Oh, Chang Ho; Rhim, Chul Yun; You, Choong Ho; Cho, Jin Rai
Synthetic Communications, 2003 , vol. 33, # 24 p. 4297 - 4302
反应条件
sodium methylate in methanol 2 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 255 - 259
反应条件
magnesium bromide in 1,4-dioxane 3 h; Heating; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 38, # 34 p. 6059 - 6062
反应条件
1: petroleum ether / 2 h / Heating 2: triethylamine / acetonitrile / 72 h / Heating 3: sodium methoxide; / methanol / 2 h View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 255 - 259
反应条件
1: triethylamine / acetonitrile / 72 h / Heating 2: sodium methoxide; / methanol / 2 h View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 255 - 259
反应条件
hydrogenchloride; triethylamine 1.) ethanol, reflux, 3 d; 2.) water, 100 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 255 - 259
反应条件
boron trifluoride diethyl etherate T=115°C;
参考文献
Journal of Organic Chemistry, , vol. 61, # 16 p. 5453 - 5455
反应条件
trifluoroacetic acid in methanol
参考文献
Gaertner,V.R.
Journal of Heterocyclic Chemistry, 1969 , vol. 6, p. 273 - 277
