2-氧-4-(三苯基膦)丁酸乙酯合成路线 (共 20 条)
反应条件
sodium hydrogencarbonate
参考文献
Chemische Berichte, , vol. 96, p. 2943 - 2949
反应条件
triphenylphosphine in tetrahydrofuran 18 h; Reflux;
参考文献
UNIVERSITE JOSEPH FOURIER; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE
Patent: US2010/298422 A1, 2010 ;
Location in patent: Page/Page column 25 ;
反应条件
NaCO3 in water 12 h; Ambient temperature;
参考文献
Sun, King Mo; Dawe, Robert D.; Fraser-Reid, Bert
Carbohydrate Research, 1987 , vol. 171, p. 35 - 48
反应条件
in toluene T=50°C; 24 h;
参考文献
Stergiou, Anastasios; Bariotaki, Anna; Kalaitzakis, Dimitris; Smonou, Ioulia
Journal of Organic Chemistry, 2013 , vol. 78, # 14 p. 7268 - 7273
反应条件
1: 2.06 percent / benzene / 72 h / Ambient temperature 2: NaHCO3 / H2O / 0 - 5 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 41, # 10 p. 1591 - 1600
反应条件
1: 97 percent / benzene / 18 h / Ambient temperature 2: 83 percent / NaCO3 / H2O / 12 h / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 171, p. 35 - 48
反应条件
sodium carbonate in water T=20°C;
参考文献
ICN Pharmaceuticals, Inc.
Patent: EP1254911 A1, 2002 ;
Location in patent: Example 52 ;
反应条件
1: With sodium methylate in methanol T=75 - 80°C; 2: With water; sodium hydroxide
参考文献
Pokhodylo; Matiychuk; Obushak
Chemistry of Heterocyclic Compounds, 2009 , vol. 45, # 12 p. 1469 - 1472
反应条件
1: With sodium methylate in methanol T=75 - 80°C; 2: With water; sodium hydroxide
参考文献
Pokhodylo; Matiychuk; Obushak
Chemistry of Heterocyclic Compounds, 2009 , vol. 45, # 12 p. 1469 - 1472
反应条件
1: With sodium methylate in methanol T=75 - 80°C; 2: With water; sodium hydroxide
参考文献
Chemistry of Heterocyclic Compounds, , vol. 45, # 12 p. 1469 - 1472