1-苯基-3-(2-甲氧基苯基)脲合成路线 （共 10 条）
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; caesium carbonate; (9,9-dimethyl-9H-xanthene-4,5-diyl)bis(bis(3,5-bis(trifluoromethyl)phenyl)phosphine) in 1,4-dioxane T=100°C; 1 h;
参考文献
Sergeev; Artamkina; Beletskaya
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 12 p. 1741 - 1752
反应条件
potassium phosphate; copper(l) iodide; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl-formamide T=85°C; 24 h;
参考文献
Gavade, Sandip N.; Balaskar, Ravi S.; Mane, Madhav S.; Pabrekar, Pramod N.; Shingare, Murlidhar S.; Mane, Dhananjay V.
Chinese Chemical Letters, 2011 , vol. 22, # 6 p. 675 - 678
反应条件
1: bis(trichloromethyl) carbonate; aniline With triethylamine in dichloromethane T=20°C; Inert atmosphere; 2: 2-methoxy-phenylamine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Charalambidis, Georgios; Ladomenou, Kalliopi; Boitrel, Bernard; Coutsolelos, Athanassios G.
European Journal of Organic Chemistry, 2009 , # 8 p. 1263 - 1268
反应条件
copper(I) oxide; potassium tert-butylate in 1-methyl-pyrrolidin-2-one T=100°C; 0.333333 h; Inert atmosphereMicrowave irradiation;
参考文献
Gavade, Sandip N.; Balaskar, Ravi S.; Mane, Madhav S.; Pabrekar, Pramod N.; Shingare, Murlidhar S.; Mane, Dhananjay V.
Chinese Chemical Letters, 2011 , vol. 22, # 3 p. 292 - 295
反应条件
copper acetylacetonate; potassium tert-butylate in 1-methyl-pyrrolidin-2-one T=20°C; 24 h; Inert atmosphereSealed vial;
参考文献
Gavade, Sandip; Balaskar, Ravi; Mane, Madhav; Pabrekar, Pramod N.; Mane, Dhananjay
Synthetic Communications, 2012 , vol. 42, # 11 p. 1704 - 1714
反应条件
in 1,4-dioxane T=100 - 110°C; 8 h; Inert atmosphere;
参考文献
Hosseinzadeh, Rahman; Sarrafi, Yaghoub; Aghili, Nora
Chinese Chemical Letters, 2010 , vol. 21, # 10 p. 1171 - 1174
反应条件
copper(I) oxide; tripotassium phosphate monohydrate T=120°C; 0.666667 h; Microwave irradiationInert atmosphereNeat (no solvent);
参考文献
Gavade, Sandip; Shingare, Murlidhar; Mane, Dhananjay
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 12 p. 4167 - 4170
参考文献
Brewster; Floyd
Trans.Kansas Acad., 1935 , vol. 38, p. 139,141,142
参考文献
Ransom
American Chemical Journal, 1900 , vol. 23, p. 39
Chemische Berichte, 1898 , vol. 31, p. 1063
参考文献
Brewster; Floyd
Trans.Kansas Acad., 1935 , vol. 38, p. 139,141,142
