反应条件
in ammonia
extraction of P4S3 with liquid NH3; heating the product in high vacuum at 275 °C then heating in a sealed tube with NH3 at 50-60 °C for 24 h; repeated extraction with NH3 and heating; removal of S under evolution of H2S;; formation of a product containing P4S(NH)2 and P4(NH)3 (ratio 1:2);;
参考文献
Behrens, H.; Huber, L.
Ber., 1960 , vol. 93, p. 921 - 927
Full Text Show Details
Gmelin Handbook: P: MVol.C, 141, page 325 - 327
