反应条件
in neat (no solvent)
Irradiation (UV/VIS); absence of air and moisture; molar ratio P4:S8=8:1, sealed tube, 150 W lamp, 0°C; then heating without irradiation to 80°C for 1 h; further products: β and γ-P4S8, α-P4S9., α-P4S5, β-P4S6, α-P4S8; not isolated, reaction followed by (31)P-NMR spectroscopy;
参考文献
Jason, Mark E.; Ngo, Toan; Rahman, Shahidur
Inorganic Chemistry, 1997 , vol. 36, # 12 p. 2633 - 2640