N-苯基吡啶-2(1H)-酮合成路线 (共 13 条)
反应条件
copper(l) iodide; potassium carbonate; N,N'-dimethylcyclohexane-1,2-diamine in toluene 18 h; Heating;
参考文献
Wang, Po-Shih; Liang, Chih-Kai; Leung, Man-Kit
Tetrahedron, 2005 , vol. 61, # 11 p. 2931 - 2939
反应条件
caesium carbonate; copper(I) oxide; trans-1,2-bis(2'-pyridylideneamino)cyclohexane in acetonitrile T=82°C; 24 h; activated 3 A molecular sieve (KnNa12,-n[(AlO2)12(SiO2)12]); Conversion of starting material;
参考文献
Cellier, Pascal Philippe; Cristau, Henri-Jean; Spindler, Jean-Francis; Taillefer, Marc
Patent: US2003/236413 A1, 2003 ;
Location in patent: Page 28 ;
反应条件
trans-N,N'-bis-[pyridin-2-ylmethylene]-cyclohexane-1,2-diamine; 3 A molecular sieve; caesium carbonate; copper(I) oxide in acetonitrile T=82°C; 24 h;
参考文献
Chemistry - A European Journal, , vol. 10, # 22 p. 5607 - 5622
反应条件
copper diacetate; tetrabutyl ammonium fluoride in tetrahydrofuran; dichloromethane T=20°C; 48 h;
参考文献
Lam, Patrick Y.S.; Vincent, Guillaume; Bonne, Damien; Clark, Charles G.
Tetrahedron Letters, 2002 , vol. 43, # 16 p. 3091 - 3094
反应条件
1: 2-Hydroxypyridine With potassium tert-butylate in tetrahydrofuran T=20°C; 0.166667 h; 2: Ph3BiCl2 in tetrahydrofuran 3 h; Heating;
参考文献
Ikegai, Kazuhiro; Mukaiyama, Teruaki
Chemistry Letters, 2005 , vol. 34, # 11 p. 1496 - 1497
反应条件
bis(1,5-cyclooctadiene)nickel (0); diethylphosphinoethane in toluene T=-20°C; 30 h;
参考文献
Hoberg, Heinz; Oster, Benno W.
Synthesis, 1982 , # 4 p. 324 - 325
反应条件
copper diacetate; triethylamine in dichloromethane 48 h;
参考文献
Meigh; Alvarez; Joule
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 17 p. 2012 - 2021
反应条件
potassium tert-butylate in tetrahydrofuran 2 h; Heating;
参考文献
Ikegai, Kazuhiro; Nagata, Yuzo; Mukaiyama, Teruaki
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 5 p. 761 - 767
反应条件
in chloroform; acetone T=70°C; 4 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 33, # 6 p. 2313 - 2322
反应条件
in chloroform; acetone T=70°C; 2 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 4 p. 1149 - 1155