in toluene byproducts: H2O; refluxing 2:1 mixt. of (C6H11)3SnOH and acid in toluene for 2 h;; azeotropical removal of H2O; recrystn. from toluene; elem. anal.;;
参考文献
Samuel-Lewis, Areila; Smith, Peter J.; Aupers, John H.; Hampson, David; Povey, David C.
Journal of Organometallic Chemistry, 1992 , vol. 437, # 1/2 p. 131 - 144
in ethanol
concd. HBr added to a soln. of Sn-compound in EtOH; mixture stirred at room temp. for 2 h; volatiles removed under vacuum; recrystallized from CHCl3;
参考文献
Howie, R. Alan; Moura, Marcelo V.H.; Wardell, James L.; Wardell, Solange M.S.V.
Polyhedron, 2004 , vol. 23, # 14 p. 2331 - 2336
