苯基 2-乙酰氨基-3,4,6-三-O-乙酰基-2-脱氧吡喃己糖苷合成路线 （共 8 条）
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane 0.75 h; Ambient temperature;
参考文献
Roy, Rene; Tropper, Francois D.
Canadian Journal of Chemistry, 1991 , vol. 69, # 5 p. 817 - 821
反应条件
1: phenyl 3,4,6-tri-O-acetyl-2-deoxy-2-N-phthalimido-β-D-glucopyranoside With ethylenediamine in butan-1-ol T=80°C; 16 h; 2: acetic anhydride With pyridine 16 h;
参考文献
Cocinero, Emilio J.; Stanca-Kaposta, E. Cristina; Dethlefsen, Mark; Liu, Bo; Gamblin, David P.; Davis, Benjamin G.; Simons, John P.
Chemistry - A European Journal, 2009 , vol. 15, # 48 p. 13427 - 13434
反应条件
tin(II) trifluoromethanesulfonate; 4 A molecular sieve; N,N,N',N'-tetramethyl-urea in dichloromethane 48 h; Ambient temperature;
参考文献
Lubineau, Andre; Gallic, Joelle Le; Malleron, Annie
Tetrahedron Letters, 1987 , vol. 28, # 42 p. 5041 - 5044
反应条件
toluene-4-sulfonic acid
参考文献
Helferich; Iloff
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1933 , vol. 221, p. 252,253, 254
Full Text Show Details
Roseman; Dorfmann
Journal of Biological Chemistry, 1951 , vol. 191, p. 607,610
反应条件
1: phenol 2: pyridine View Scheme
参考文献
Helferich et al.
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1934 , vol. 226, p. 258,261
反应条件
1: pyridine 2: acetic acid anhydride; hydrogen chloride 3: acetone; aq. NaOH solution View Scheme
参考文献
Leaback; Walker
Journal of the Chemical Society, 1957 , p. 4754,4757
反应条件
1: phenol 2: pyridine View Scheme
参考文献
Helferich et al.
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1934 , vol. 226, p. 258,261
反应条件
1: acetic acid anhydride; hydrogen chloride 2: acetone; aq. NaOH solution View Scheme
参考文献
Leaback; Walker
Journal of the Chemical Society, 1957 , p. 4754,4757
