3-(溴甲基)-5-甲基异恶唑合成路线 （共 5 条）
反应条件
PPh3.Br2 in dichloromethane 1 h; Ambient temperature;
参考文献
Pei; Wickhan
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7509 - 7512
反应条件
1: 60 percent / LiAlH4 / tetrahydrofuran / 0.5 h / -78 °C 2: 65 percent / Ph3PBr2 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 47 p. 7509 - 7512
反应条件
1: 74 percent / NH2OH*HCl / ethanol / 2 h / Heating 2: 60 percent / LiAlH4 / tetrahydrofuran / 0.5 h / -78 °C 3: 65 percent / Ph3PBr2 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 47 p. 7509 - 7512
反应条件
sodium azide in acetone 24 h; Ambient temperature;
参考文献
Pei; Wickhan
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7509 - 7512
反应条件
1: 84 percent / NaN3 / acetone / 24 h / Ambient temperature 2: 98 percent / NaBH4, TEA / HS(CH2)3SH / propan-2-ol / 24 h / Ambient temperature View Scheme
参考文献
Pei; Wickhan
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7509 - 7512
