反应条件
1: 1.) Mg, I2 / 1.) ethanol, 2.) reflux, 30 h 2: NaH, 18-crown-6 / 1.) toluene, r.t., 1 h, 2.) toluene, reflux, 24 h 3: 15percent aq. NaOH / 40 h / Heating 4: 85 percent / KOH, hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 1.) 140 deg C, 2.) 190-200 deg C, 5 h View Scheme
参考文献
Naoshima; Ozawa; Takenami; et al.
Agricultural and Biological Chemistry, 1981 , vol. 45, # 7 p. 1723 - 1724
