3-甲氧基-2-萘甲酸甲酯合成路线 （共 25 条）
反应条件
1: LiAlH4; diethyl ether
3: LiAlH4; THF
4: pyridine hydrochloride
5: acetic acid; CHCl3; lead (IV)-acetate
6: aqueous acetic acid
View Scheme
参考文献
Ebnoether et al.
Helvetica Chimica Acta, 1952 , vol. 35, p. 910,926
反应条件
1: 93 percent / LiAlH4 / tetrahydrofuran / 3 h / 20 °C
2: 92 percent / 4-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH2Cl2
View Scheme
参考文献
Wu, Kun-Chan; Lin, Yu-Shan; Yeh, Yu-Shan; Chen, Chun-Yen; Ahmed, Moawia O.; Chou, Pi-Tai; Hon, Yung-Son
Tetrahedron, 2004 , vol. 60, # 51 p. 11861 - 11868
反应条件
1: 87 percent / LiAlH4 / tetrahydrofuran / 6 h / 20 °C
2: 82 percent / pyridinium chlorochromate; sodium acetate; molecular sieves 4 Angstroem / CH2Cl2 / 0.67 h
3: 80 percent / BBr3 / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Wu, Kun-Chan; Lin, Yu-Shan; Yeh, Yu-Shan; Chen, Chun-Yen; Ahmed, Moawia O.; Chou, Pi-Tai; Hon, Yung-Son
Tetrahedron, 2004 , vol. 60, # 51 p. 11861 - 11868
反应条件
1: sodium; diethyl ether
2: hydrogen bromide; acetic acid
View Scheme
参考文献
Virkar; Wheeler
Journal of the Chemical Society, 1939 , p. 1679
反应条件
1: 99 percent / LiAlH4 / diethyl ether / 12 h / Heating
2: 97 percent / hydrogen / Pd/C / ethyl acetate / 7.5 h
View Scheme
参考文献
Ebnoether et al.
Helvetica Chimica Acta, 1952 , vol. 35, p. 910,926
