反应条件
in 2-methyl cyclohexane N2 atm.; cooling (1 h, -78°C), stirring (room temp., 72 h); extraction (toluene (30°C, 30 torr), acetonitrile (vac.)), concn.(0.05 torr, 25°C), centrifugation, crystn. (PhMe/CH3CN, 10/1-1/3 );
参考文献
Gereke, Robert; Plinta, Hans-Juergen; Schmutzler, Reinhard
Zeitschrift fur Anorganische und Allgemeine Chemie, 1997 , vol. 623, # 8 p. 1333 - 1343
